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- E-ISSN 2288-8985
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Simultaneous determination of aromatic material causing allergic in children’s products by Gas Chromatography
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2018, v.31 no.1, pp.23-30
https://doi.org/10.5806/AST.2018.31.1.23
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(2018). Simultaneous determination of aromatic material causing allergic in children’s products by Gas Chromatography. Analytical Science and Technology, 31(1), 23-30, https://doi.org/10.5806/AST.2018.31.1.23
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Abstract
Twenty-two allergy-induced aromatics in children were analyzed using a gas chromatography flame ionization detector (GC-FID) and gas chromatography mass spectrometer (GC-MSD). Analytes were extracted using an automatic Soxhlet extractor and centrifuged for 10 min in a fast freezing centrifuge, and the supernatant was transferred into a 2 mL vial and injected in split mode. Under the established conditions, the calibration curve showed linearity with a correlation coefficient of 0.996 or more. A wide range of sensitivity of 6.7 to 1,859,839 depending on the device characteristics and detector used was shown. The detection limit of the device was 0.0032 to 0.0335 μg/mL, and the maximum detection limit was less than 0.1 μg/mL. The detection limit of the method ranged from 0.0033 to 0.1161 μg/mL. In addition, the limit of quantification ranged from 0.0100 to 0.5422 μg/mL, with a level of precision ranging from 0.21 % to 4.89 % and a degree of accuracy ranging from 89 % to 111 %. The analytical method developed in this study was applied to commercial products.
- keywords
- allergy, aromatic material, children's products, GC-FID, GC-MSD
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