- P-ISSN 1225-0163
- E-ISSN 2288-8985
- P-ISSN1225-0163
- E-ISSN2288-8985
- SCOPUS, ESCI, KCI
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Study on simultaneous determination of aromatic material causing allergic in children’s products by GC-MSD
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2020, v.33 no.3, pp.134-142
https://doi.org/10.5806/AST.2020.33.3.134
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(2020). Study on simultaneous determination of aromatic material causing allergic in children’s products by GC-MSD. Analytical Science and Technology, 33(3), 134-142, https://doi.org/10.5806/AST.2020.33.3.134
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Abstract
Twenty-one allergy-induced aromatic material in children’s products were analyzed using gas chromatography mass spectrometer(GC-MSD). The analytes were extracted using an automatic Soxhlet extractor, centrifuged for 10 minutes in a fast freezing centrifuge, and the supernatant was filtered with a syringe filter and then transferred into a 2 mL vial and injected in a split mode. In the established condition, the calibration curve showed linearity with a determination coefficient of 0.9981 or more. Sensitivity was 0.3145 ~ 1.6757, which showed a fairly wide range of sensitivity for each substance. The detection limit of the device was 0.0016 ~ 0.0423 μg/mL and the maximum detection limit was less than 0.05 μg/mL. The method detection limit ranged from 0.0030 ~ 0.0589 μg/mL. In addition, the limit of quantification ranged from 0.0096 to 0.1876 μg/mL, with precision ranging from 0.41 to 10.49 % and accuracy ranging from 83 to 116 %. The analytical method developed in this study was applied to commercial products.
- keywords
- allergy, aromatic material, children's products, fragrance, GC-MSD
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