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- E-ISSN 2288-8985
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A study on development of CRM by means of XRF analysis for fine ceramic (<TEX>$BaTiO_3$</TEX>)
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
1996, v.9 no.4, pp.382-391
Kim,
Y. M., Jeong,
C. Y., Lim,
C. H., Song,
T. Y., &
Lee,
D.
S.
(1996). A study on development of CRM by means of XRF analysis for fine ceramic (<TEX>$BaTiO_3$</TEX>). Analytical Science and Technology, 9(4), 382-391.
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Abstract
In this study, 12 different chemical species of fine ceramic(<TEX>$BaTiO_3$</TEX>) were synthesized as the standard materials for the fast and accurate measurements of X-ray fluorescence spectrometry. Samples were diluted to sixteen times with the filling compound (<TEX>$Li_2B_4O_7+LiBO_2$</TEX>) in order to remove the matrix effect, and to get the convenient storage and homogeneity of ingredients. The matrix effects among the ingredients were corrected by the empirical coefficient method based on the Lucas-Tooth and Price model. The standard curve on 12 standard materials containing 15 elements were obtained by using X-ray fluorescence spectrometry at three different laboratories. The correlation factors of BaO, PbO, SrO, <TEX>$Fe_2O_3$</TEX>, <TEX>$La_2O_3$</TEX>, <TEX>$SnO_2$</TEX>, ZnO, <TEX>$ZrO_2$</TEX>, CaO indicated the relati vely good agreement over 0.995 among the three different laboratories. <TEX>$SiO_2$</TEX> and <TEX>$Al_2O_3$</TEX> showed the poor linearity because of their low fluorescence intensities.
- keywords
- Barium Titanate, X-ray Fluorescence Sectroscopy, Glass Bead Method
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