- P-ISSN 1225-0163
- E-ISSN 2288-8985
- P-ISSN1225-0163
- E-ISSN2288-8985
- SCOPUS, ESCI, KCI
Article Detail
Home > Article Detail
Determination of Polybrominated Biphenyls in Biota Samples Using Gas Chromatography/Mass Spectrometry
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2000, v.13 no.5, pp.666-674
Hong,
J., Baek,
I., Kim,
H., Kim,
D., Seo,
J., Seo,
J., Park,
H., &
Lee,
K.
(2000). Determination of Polybrominated Biphenyls in Biota Samples Using Gas Chromatography/Mass Spectrometry. Analytical Science and Technology, 13(5), 666-674.
- Downloaded
- Viewed
Abstract
The present study describes an analytical method for the determination of polybrominated biphenyls (PBBs) in biota samples by gas chromatography-mass spectrometry (GC/MS). PBBs are extracted twice from 20 g samples with mixture solvent 40mL acetone and 80mL hexane using ultrasonic agitation for 20 min. Lipids in extracts are degraded by concentrated sulfuric acid and then PBBs are purified with Florisil column. The purified extracts are analyzed by GC/MS-selected ion monitoring mode for the quantitation of PBBs in biota sample. The overall recovery yields of PBBs range between 77 and 111% under these experimental conditions.
- keywords
- PBBs, clean-up, biota sample, GC/MS-SIM
- Downloaded
- Viewed
- 0KCI Citations
- 0WOS Citations
Other articles from this issue
- Uncertainty in Measurements and Analyses ( 4 ) - Expression and Calculation of Uncertainty by the International Rule ( GUM ) -
- The Hydrolysis Measurement of Cyclodextrins Using FTIR-ATR Spectrometry
- Properties of Mononuclear and Binuclear Cu(II) Schiff Base Complexes and Oxidation of Ascorbic Acid
- A Study on the Standards for Xe Analysis by Wavelength Dispersive X-ray Spectrometer (WDS) of Electron Probe Micro Analysis (EPMA)
- Liquid Phase Adsorption of Activated Carbon Fibers
- A Study on the Separation of Neodymium from the Simulated Solution of <TEX>$U_3Si/Al$</TEX> Spent Nuclear Fuel
- Simultaneous Determination of Biliary Free and Phospholipid Fatty Acids Using Gas Chromatography-Mass Spectrometry
- Determination of La in <TEX>$U_3Si/Al$</TEX> Spent Nuclear Fuel by Ion Chromatography-Inductively Coupled Plasma-Mass Spectrometry
- Preconcentration and Determination of Trace Cobalt and Nickel by the Adsorption of Metal-PDC Complexes on the Anion-Exchange Resin Suspension
- Determination of Phthalate Esters and Adipate in Water and Sediment Samples
- Homogeneous Enzyme-linked Binding Assay for Mistletoe Lectin I Based on the Mistletoe Lectin I/D-galactose Interaction
- Effects of Some Crude Drug Extracts on the Brain Neurotransmitters in the Ethanol-Treated Rats
- The Extraction and Derivatization of Organotins in Water Sample by Gas Chromatograph/Mass Spectrometer
- Photocatalytic Destruction of a Mordant Yellow-12 Using Rutile-<TEX>$TiO_2$</TEX>
- Degradation of Humic Acids by Ozone/high pH, Ozone/Hydrogen Peroxide and Ozone/Hydrogen Carbonate System
- Formation of Hydrogen Peroxide by the Ozonation of Aqueous Humic Acid
- Determination of Polybrominated Biphenyls in Biota Samples Using Gas Chromatography/Mass Spectrometry
- Certification and Quality Control of the Official Test Facilities of Dioxins in Korea
- The Volatile Organic Compounds Released from PVC Food Wrapping Film at Normal Use Condition
- Uncertainty in Measurements and Analyses(IV) - Expression and Calculation of Uncertainty by the International Rule(Gum) -
- more
Recommanded Articles
This website recommended the use the Chrome browser for journal website.