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Synthesis and Analysis of 6,6-dichlorobicyclo[3, 1, 0]hexane-3-carboxylic acid
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2001, v.14 no.1, pp.1-7
Lee,
K., &
Yang,
J.
(2001). Synthesis and Analysis of 6,6-dichlorobicyclo[3, 1, 0]hexane-3-carboxylic acid. Analytical Science and Technology, 14(1), 1-7.
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Abstract
6,6-Dichlorobicyclo[3, 1, 0]hexane-3carboxylic acid was synthesized by dichlorocarbene addition into 3-cyclopentenecarboxylic acid using BTEA.Cl as phase transfer catalyst. <TEX>$^1H$</TEX> NMR <TEX>$^{13}C$</TEX> NMR data analyst showed that this compound had boat-like conformation and carboxyl group existed as trans form.
- keywords
- dichlorocarbene addition, PTC, <TEX>$^{13}C$</TEX> NMR
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