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- E-ISSN 2288-8985
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Determination of Plasticizers included in Balloon by Solid Phase Microextraction and Gas Chromatography with Mass Spectrometric Detection
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2001, v.14 no.1, pp.44-49
Park,
H., Kim,
J., Ryu,
J., Kim,
Y., &
Lee,
K.
(2001). Determination of Plasticizers included in Balloon by Solid Phase Microextraction and Gas Chromatography with Mass Spectrometric Detection. Analytical Science and Technology, 14(1), 44-49.
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Abstract
Solid-phase microextraction (SPME) with <TEX>$85{\mu}m$</TEX> polyacrylate fiber, coupled to gas chromatography-mass spectrometry was used to analyze the plasticizers contained in balloon samples. The balloons were identified to be made of polyisoprene by IR spectroscopy. The plasticizers extracted from the balloon samples soaked in acetone-added water solvent for an hour were quantified by external standard method using nine kinds of plasticizers. The quantification method was validated for standard plasticizers in the range of <TEX>$0.25-25{\mu}g/g$</TEX>. The detection limits were <TEX>$0.11-0.38{\mu}g/g$</TEX> for different plasticizers. The RSDs for the reproducibility of this quantitation method were 3.7-14.2%. A few of balloons included risky level of plasticizer concerned as and endocrine disrupter, and it is necessary to regulate these products.
- keywords
- plasticizers, phthaIates, baIloon analysis, GC-MS, SPME
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