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Separation of Plutonium Oxidation States by Ion Chromatography
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2001, v.14 no.1, pp.28-33
Kim,
S. S., Jun,
K. S., &
Kang,
C.
H.
(2001). Separation of Plutonium Oxidation States by Ion Chromatography. Analytical Science and Technology, 14(1), 28-33.
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Abstract
The ion chromatography for the separation of plutonium species which are suggested to be <TEX>$Pu^{3+}$</TEX>, <TEX>$Pu^{4+}$</TEX>, <TEX>$PuO_2{^+}$</TEX> and <TEX>$PuO_2{^{2+}}$</TEX> in natural water was studied. Two separation methods were performed; 1) two-column method containing each of <TEX>$SiO^-$</TEX> and SiO-<TEX>$SO_3{^-}$</TEX> cation exchanger, 2) IC with AG11 column and the eluent of oxalate/nitric acid. Separation conditions for <TEX>$Eu^{3+}$</TEX>, <TEX>$Th^{4+}$</TEX>, <TEX>$NpO_2{^+}$</TEX>, <TEX>$UO_2{^{2+}}$</TEX> in place of plutonium species were acquired from preliminary tests. When these conditions were applied to separate the plutonium species, two-column method was separated them successfully. However, the IC method with oxalate eluent was difficult in the separation of plutonium species due to the change of <TEX>$Pu^{3+}$</TEX> and <TEX>$PuO_2{^{2+}}$</TEX> to <TEX>$Pu^{4+}$</TEX> and <TEX>$PuO_2{^+}$</TEX> respectively.
- keywords
- plutonium, separation, chromatography, ion exchanger, oxalate
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