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  • P-ISSN1225-0163
  • E-ISSN2288-8985
  • SCOPUS, ESCI, KCI

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  • P-ISSN 1225-0163
  • E-ISSN 2288-8985

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    유통 화장품 중 내분비계 장애물질 탐색 및 규명에 관한 연구

    The analysis of endocrine distruptors in commercial cosmetics

    분석과학 / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
    2015, v.28 no.3, pp.212-220
    https://doi.org/10.5806/AST.2015.28.3.212
    구희수 (부산광역시보건환경연구원)
    나영란 (부산광역시보건환경연구원)
    이승주 (부산광역시 보건환경연구원)
    민상기 (부산광역시 보건환경연구원)
    강정미 (부산광역시 보건환경연구원)
    진성현 (부산광역시 보건환경연구원)
    구희수, 나영란, 이승주, 민상기, 강정미, & 진성현. (2015). 유통 화장품 중 내분비계 장애물질 탐색 및 규명에 관한 연구. 분석과학, 28(3), 212-220, https://doi.org/10.5806/AST.2015.28.3.212
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    Abstract

    This study aims to identify the characteristics of phthalates (DMP, DEP, DBP, DEHA, BBP, DEHP, and DNOP) and heavy metals such as lead (Pb), cadmium (Cd), and mercury (Hg) in cosmetics and their containers. Phthalates and heavy metals may be endocrine distruptors. Sixty-five cosmetics were purchased from online and offline stores in Busan. This study developed a simultaneous method for the analysis of phthalates by GC-FID. The results showed that among the 65 cosmetics, DBP, DEHP, and DEP were detected at 20.0%, 7.7%, 1.5%, respectively. The amounts of DBP and DEHP detected in 18 samples were less than 100 μg/g, which satisfies the Regulations of Cosmetic Safety Standards in Korea. In order to detect phthalates in cosmetic containers, a dissolution test was conducted by extracting solutions, such as water, n-heptane, 20% ethanol, 50% ethanol and 4% acetic acid, which were prepared with different levels of pH, alcohol content, and fat content following the Korea Standards and Specifications for Utensils, Containers, and Packaging. The results showed that DMP, DBP, DEHA, BBP, DEHP, and DNOP were not detected, DEP was detected in plastics such as PE, PP, and others, when a 50% alcohol solvent was used. Phthalates may not be detected in cosmetic containers if they are not packaged with the above 20% alcohol constituent. We also analyzed the concentration of heavy metals, such as Pb, Cd, and Hg, by using ICP-OES and a mercury analyzer. The ranges of concentration were ND~2.71 μg/g for Pb, ND~0.31 μg/g for Cd, and ND~0.01 μg/g for Hg, which are below the regulated level.

    keywords
    cosmetics, phthalate, heavy metal, endocrine disruptors, GC-FID


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