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Analysis of animal glue by pyrolysis/GC/MS
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2015, v.28 no.3, pp.221-227
https://doi.org/10.5806/AST.2015.28.3.221
(2015). Analysis of animal glue by pyrolysis/GC/MS. Analytical Science and Technology, 28(3), 221-227, https://doi.org/10.5806/AST.2015.28.3.221
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Abstract
아교는 불화, 단청, 나전의 접착제 등 문화재에서 접착제로 광범위하게 사용되어 온 전통재료이다. 아교의 분석과 확인은 주로 IR 등의 분광학적인 방법으로 이루어져 왔으나, 아교의 성분을 확인하는데 어려움이 있다. 열분해/GC/MS분석은 시료의 열분해 산물을 통해 시료의 성분을 추정할 수 있어합성수지 등 고분자 재료의 성분을 분석하는데 유용하다. 본 연구에서는 아교의 화학 성분을 파악하기위한 기초 단계로서 열분해/GC/MS분석을 시도하였다. 열분해 온도, 시료량, 반복성과 같은 분석 조건을검토하여 적절한 분석이 가능한 조건을 찾았고, 이 조건에서 아교의 열분해 산물을 일부 규명하였다. 또한, 국내외에서 시판되는 젤라틴과 아교의 열분해 분석을 통해 아교와 젤라틴, 아교와 아교 사이에 제품에 따른 열분해 산물 차이가 없음을 확인하였다. 이로부터 문화재에서 아교의 사용 여부를 확인하기위한 분석법의 제시와 아교를 젤라틴으로 대체하는데 필요한 화학성분상의 기초자료 확보가 가능하였다.
- keywords
- animal glue, cultural heritage, pyrolysis/GC/MS, gelatin
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