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A Study on the Precursor of <TEX>$BaTiO_3$</TEX> Synthesized in Water
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
1992, v.5 no.4, pp.409-415
Kim,
S., Huh,
W. Y., &
Lee,
C.
(1992). A Study on the Precursor of <TEX>$BaTiO_3$</TEX> Synthesized in Water. Analytical Science and Technology, 5(4), 409-415.
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Abstract
Factor analysis was applied to X-ray diffraction patterns of the precursor of <TEX>$BaTiO_3$</TEX>. For that purpose, the precursor was synthesized in water solvent system using <TEX>$Ba(NO_3)_2$</TEX> and <TEX>$TiO(NO_3)_2$</TEX> as the starting materials and calcined at various temperatures. The samples obtained from the various calcined temperatures were analyzed by the X-ray diffractometer. Factor analysis was applied to the intensity data of the X-ray diffraction patterns. As the results, three factors were found and they were found to be <TEX>$BaCO_3$</TEX>, <TEX>$BaTiO_3$</TEX> and <TEX>$Ba_2TiO_4$</TEX>. The relative concentrations of the three components were estimated during calcination.
- keywords
- <TEX>$BaTiO_3$</TEX>, factor analysis, X-ray diffraction patterns
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