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Synthesis and Analytical Application of Piperidine Dithiocarbamate Complex of Copper(II)
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
1999, v.12 no.1, pp.1-6
Kim,
C., &
Kim,
C.
(1999). Synthesis and Analytical Application of Piperidine Dithiocarbamate Complex of Copper(II). Analytical Science and Technology, 12(1), 1-6.
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Abstract
Copper(II) complex of piperidine dithiocarbamate (Pipdtc) was synthesized from the reaction of Cu(II) and piperidine dithiocarbamate. The possible structure of the complex was proposed on the basis of elemental analysis, molar conductivity, infrared spectroscopy, electronic absorption spectroscopy, and <TEX>$^{13}C-NMR$</TEX> studies. The extraction of copper(II)-Pipdtc complex by carbon tetrachloride can be achieved in the pH range of 6.0~10. The solution of copper(II) with piperidine dithiocarbamate was bey Beer's law in the concentration up to <TEX>${\sim}8.0{\times}10^{-5}M$</TEX> at pH 9.0.
- keywords
- piperidine dithiocarbamate complex, <TEX>$^{13}C-NMR$</TEX>, <TEX>$CCl_4$</TEX> extraction
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