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- E-ISSN 2288-8985
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Property analysis of polysilane precursors and applications for polysilicon
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2012, v.25 no.6, pp.345-349
https://doi.org/10.5806/AST.2012.25.6.345
(2012). Property analysis of polysilane precursors and applications for polysilicon. Analytical Science and Technology, 25(6), 345-349, https://doi.org/10.5806/AST.2012.25.6.345
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Abstract
Polysilane black powders were synthesized by sonochemical methods from silicon tetrachloride with sodium metal with 37.0% yield. Those black powder materials were found to have fibrous or irregular shapes with round surface. It was found that thermal behaviors of those polysilane black powders were similar to that of hydropolysilanes which was reported earlier. After thermal treatment, black polysilicon was obtained with 57.1% residue yield, and those fibrous or irregular shapes with round surface were intact but lots of small cavities were formed indicating porous structure, and found to be an amorphous state from XRD analysis.
- keywords
- polysilane black powder, sonochemical synthesis
Reference
1
1. S.-A. Ahn, S.-H. Lee, Y. S. Song and G.-H. Lee, Anal. Sci. Tech. 24, 105 (2011).
2
2. E.-O. Yang, J.-K. Lee, S.-H. Lee, Y. S. Song and G.-H. Lee, Anal. Sci. Tech. 19, 504 (2006).
3
3. H. K. Kim and K. Matyjaszewski, J. Am. Chem. Soc., 110, 3321 (1988).
4
4. K. Matyjaszewski, D. Greszta, S. H. Jeffrey and H. K. Kim, Macromolecules, 28, 59. (1995).
5
5. R. Kani, Y. Nakano, H. Yoshida, S. Mikoshiba and S. Hayase, J. Polymer Sci.: Pare A. Polym. Chem., 35, 2355 (1997).
6
6. R. D. Miller, D. Thomson, R. Sooriyakumaran and G. N. Fickes, J. Polym. Sci.; Part A, Polym. Chem., 29, 813 (1991).
7
7. M. Suzanne, W. Bushnell, J. M. Michael and H. S. John, Polymer, 37, 2067 (1996).
8
8. T. Shimoda, S. Miyashita, S. Seki, M. Furusawa, I. Yudasaka, Y. Takeuchi and Y. Matsuki, U. S. Patent 6541354 B1 (2003).
9
9. T. Shimoda, Y. Matsuki, M. Furusawa, T. Aoki, M. Yudasaka, H. Tanaka, H. Iwasawa, D. Wang, M. Miyasaka and Y. Takeuchi, Nature, 440, 783 (2006).
10
10. H. Shiho and H. Kato, U. S. Patent 0185712 A1 (2006).
11
11. S. H. Jang, C. K. Park, Y. S. Song and G.-H. Lee, Bull. Korean Chem. Soc., 17, 443 (1996).
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