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- E-ISSN 2288-8985
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- E-ISSN2288-8985
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Development of the testing method for vinyl chloride monomer (VCM) in polyvinyl chloride(PVC) samples
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2012, v.25 no.6, pp.395-401
https://doi.org/10.5806/AST.2012.25.6.395
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(2012). Development of the testing method for vinyl chloride monomer (VCM) in polyvinyl chloride(PVC) samples. Analytical Science and Technology, 25(6), 395-401, https://doi.org/10.5806/AST.2012.25.6.395
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Abstract
This study presents a method for the quantitative analysis of residual vinyl chloride monomer (VCM)in PVC products. In elution solvent, the extraction efficiency was similar by ethanol, THF, and acetone, but using n-hexane, it indicated relatively low extraction efficiency. Measuring VCM in the pulverized PVC samples, it showed reasonable results in both the direct injection method and headspace method with GC/MS. Regarding analysis of VCM in the intermediate sponge samples, five laboratories showed good results, and from the results, it was considered that VCM quantitative method in this study was reliable.
- keywords
- vinyl chloride monomer, polyvinyl chloride, plastics, test method
Reference
1
1. The Vinyl Institute; http://www.vinylinfo.org/aboutvi/vi_commitment2.html
2
2. KS K 0730, Test method for residual vinyl chloride monomer(VCM) content of poly(vinyl chloride) fiber and resins, Korean Agency for Technologys and Standards, 2009.
3
3. EPA method 5021, Volatile organic compounds in soils and other solid matrices using equilibrium headspace analysis, US Environmental Protection Agency, 1996.
4
4. ISO 8762, Workplace-Determination of vinyl chloride charcoal tube/gas chromatographic method, International Organization for Standardization, 1988.
5
5. ASTM D 3680, Standard Test Method for Residual Vinyl Chloride Monomer Content of Poly(Vinyl Chloride) Resins, Compounds, and Copolymers by Solution Injection Technique, American Society for Testing and Materials, 2005.
6
6. ASTM D 3749, Standard Test Method for Residual Vinyl Chloride Monomer in Poly(Vinyl Chloride) Resins by Gas Chromatographic Headspace Technique, American Society for Testing and Materials, 2008.
7
7. Ministry of Knowledge Economy, http://www.mctnet.org/index.jsp
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