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Determination of phenol using solid-phase extraction and HPLC/MSD/FLD in water
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2015, v.28 no.6, pp.370-376
https://doi.org/10.5806/AST.2015.28.6.370
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(2015). Determination of phenol using solid-phase extraction and HPLC/MSD/FLD in water. Analytical Science and Technology, 28(6), 370-376, https://doi.org/10.5806/AST.2015.28.6.370
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Abstract
An analytical method for determining phenol considered priority pollutants of the US EPA and precursor of toxic phenolic compounds by solid-phase extraction (SPE) and high performance liquid chromatographic systems (HPLC) equipped with fluorescence and mass selective detectors have been developed. The SPE process for sample preconcentration was performed on a commercially available Oasis HLB cartridge packed with polymeric sorbents. The effect of pH, elution solvent, and elution volume on the recoveries of the analytes were investigated with HPLC/FLD. Average recovery of >87.0% was achieved with 60 mg sorbents using 5 mL of methanol as an elution solvent at pH=3.
- keywords
- phenol, hplc, solid phase extraction(spe), hplc/msd
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