- P-ISSN 1225-0163
- E-ISSN 2288-8985
- P-ISSN1225-0163
- E-ISSN2288-8985
- SCOPUS, ESCI, KCI
Article Detail
Home > Article Detail
Evaluation of proficiency and improvement of accuracy on the analysis of brominated flame retardants (PBDEs) in ABS polymer
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2015, v.28 no.6, pp.446-452
https://doi.org/10.5806/AST.2015.28.6.446
&
(2015). Evaluation of proficiency and improvement of accuracy on the analysis of brominated flame retardants (PBDEs) in ABS polymer. Analytical Science and Technology, 28(6), 446-452, https://doi.org/10.5806/AST.2015.28.6.446
- Downloaded
- Viewed
Abstract
In order to evaluate and improve the ability of Korean testing laboratories to measure Polybrominated diphenyl ethers in acrylonitrile-butadiene-styrene (ABS), a proficiency test was organised by Korea Research Institute of Standards and Science (KRISS) based on ISO/IEC 17043. The proficiency test material used was 10 g of a granular ABS fortified with a mixture of congeners of PBDE (BDE-154, 183, 206, 209). Homogeneity and stability were investigated to assess the adequacy of the test material. The certified value established by KRISS based on the national reference was used for assigned value of each PBDE. The test materials were distributed to the 16 participating laboratories. The participating laboratories were requested to analyse the samples employing the methods used in their routine analysis. Each laboratory was given it’s own code to secure the anonymity. Participants results were evaluated with z-scores according to ISO/IEC 17043. The standard deviation for proficiency assessment was set by standard deviation of the participants results except for outlier. The results, the laboratory's performance and improvement of accuracy were discussed.
- keywords
- acrylonitrile-butadiene-styrene (ABS), proficiency test, flame retardants, polybrominated diphenyl ether (PBDE)
Reference
1
1. M. Riess, T. Ernst, R. Popp, B. Muller, H. Thoma, O. Vierle, M. Wolf and R. van Eldik, Chemosphere, 40, 937-941 (2000).
2
2. A. Sepúlveda, M. Schluep, F. G. Renaud, M. Streicher, R. Kuehr, C. Hagelüken and A. C. Gerecke, Environ. Impact. Assess. Rev., 30, 28-41 (2010).
3
3. European Union, Official J. Eur. Union., L37, 24-38 (2003).
4
4. European Union, Official J. Eur. Union, L37, 19-23 (2003).
5
5. H. Hirai, H. Takada and Y. Ogat, Mar. Pollut. Bull., 62, 1683-1692 (2011).
6
6. F. Vilaplanaa, P. Karlsson, A. Ribes-Greus, P. Ivarsson and S. Karlsson, J. Chromatogr. A, 1196-1197, 139-146 (2008).
7
7. F. Vilaplanaa, A. Ribes-Greus and S. Karlsson, Talanta, 78, 33-39 (2009).
8
8. M. Schlummer, F. Brandl, A. Maurer and R. van Eldik, J. Chromatogr. A, 1064, 39-51 (2005).
9
9. D. Kim, J. Ryu and Y. Choi, Anal. Sci. Tech., 24(6), 435-442 (2011).
10
10. The International Organization for Standardization, ISO Guide 35, ‘Reference materials-General and statistical principles for certification’, 3rd Ed., 2006.
11
11. The International Organization for Standardization, ISO/ IEC 17043, ‘Conformity assessment-General requirements for proficiency testing’, 1st Ed., 2010.
12
12. R. Zeleny, S. Voorspoels, M. Ricci, R. Becker, C. Jung, W. Bremser, M. Sittidech, N. Panyawathanakit, W. F. Wong, S. M. Choi, K. C. Lo, W. Y. Yeung, D. H. Kim, J. Han, J. Ryu, S. Mingwu, W. Chao, M. M. Schantz, K. A. Lippa, S. Matsuyama, Anal Bioanal Chem, 396, 1501-1511 (2010).
13
13. International Electrotechnical Commission, IEC 62321, ‘Electrotechenical products-Determination of levels of six regulated substances’, Edition 1.0, 2008.
14
14. The International Organization for Standardization, ISO/ 5725-2, ‘Accuracy (trueness and precision) of measurement methods and results-Part 2’, 1st Ed., 1994.
Other articles from this issue
- Regulatory mechanism of Angelica Gigas extract powder on matrix metalloproteinases in vitro and in vivo model
- Determination of phenol using solid-phase extraction and HPLC/MSD/FLD in water
- Status of a national monitoring program for environmental radioactivity and investigation of artificial radionuclide concentrations (134Cs, 137Cs and 131I) in rivers and lakes
- Establishment of analytical methods for HPHC list of mainstream cigarette smoke
- A case study of verifying a suicide by carbon monoxide intoxication committed by burning an ignition charcoal briquette
- Improvement of analytical methods for arsenic in soil using ICP-AES
- A study of relationship between stomach cancer and selenoproteins in Korean human blood serum
- Development of a cholesterol biosensor modified with carbon nanotube
- Two dimensional analysis between the performance and the sensitivity of methylnitroimidazole derivatives
- Analysis of volatile compounds and metals in essential oil and solvent extracts of Amomi Fructus
- Evaluation of proficiency and improvement of accuracy on the analysis of brominated flame retardants (PBDEs) in ABS polymer
- Optimization of fractionation efficiency (FE) and throughput (TP) in a large scale splitter less full-feed depletion SPLITT fractionation (Large scale FFD-SF)
- Quantitative analysis of cholesterol in infant formula by isotope dilution liquid chromatography-tandem mass spectrometry
- more
Recommanded Articles
This website recommended the use the Chrome browser for journal website.