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Analysis of volatile aroma compounds from vanilla perfume using headspace disk type monolithic material sorptive extraction
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2011, v.24 no.6, pp.421-428
https://doi.org/10.5806/AST.2011.24.6.421
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(2011). Analysis of volatile aroma compounds from vanilla perfume using headspace disk type monolithic material sorptive extraction. Analytical Science and Technology, 24(6), 421-428, https://doi.org/10.5806/AST.2011.24.6.421
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Abstract
In this study, headspace disk type monolithic material sorptive extraction (HS-MMSE) was developed,validated and applied to the analysis of volatile aroma compounds from vanilla perfume by gas chromatography -mass spectrometry (GC/MS). HS-MMSE uses monolithic material (MonoTrap) based on silica bonded with octadecyl silane (ODS) and activated carbon as a sorbent. Aroma compounds was adsorbed onto the MonoTrap in headspace and extracted by only 100 μL of solvent. Total 12 volatile compounds from vanilla perfume were successfully analyzed using HS-MMSE. The influence of extractive parameters was investigated and optimized,using benzyl acetate, linalyl acetate, vanillin, ethyl vanillin as target compounds. Under the optimum condition,the limit of detection (S/N = 3) and the limit of quantification (S/N = 10) of proposed method for the target compounds were obtained within the range of 8.35~13.76 ng and 27.82~45.88 ng, respectively. The method showed good linearity with correlation coefficient more than 0.9888, satisfactory recovery and reproducibility. These results showed that HS-MMSE using disk type MonoTrap is a new promising technique for the analysis of volatile aroma compounds from vanilla perfume.
- keywords
- monolithic material, MonoTrap, GC/MS, vanilla perfume, aroma
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