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Analytical study on nickel content in ceramic, metal and plastic materials
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2011, v.24 no.6, pp.443-450
https://doi.org/10.5806/AST.2011.24.6.443
(2011). Analytical study on nickel content in ceramic, metal and plastic materials. Analytical Science and Technology, 24(6), 443-450, https://doi.org/10.5806/AST.2011.24.6.443
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Abstract
Quantitative analytical condition for nickel in ceramic, metal and plastic materials using complexation and solvent extraction followed by inductively coupled plasma-atomic emission spectrometry (ICP-AES) and atomic absorption spectrophotometry (AAS) was studied. Ceramic, metal and plastic samples were dissolved by acid digestion. Nickel was determined by ICP-AES and AAS after extraction of Ni (DMG)_2 in CHCl_3. Recovery efficiency of nickel was satisfactory, and most of matrix elements causing interference could be effectively eliminated by the separation. Nickel in the certified reference materials (BAM-376 and PACS-2)were quantitatively determined without influence of sample matrix.
- keywords
- nickel, chelation, dimethylglyoxime, solvent extraction, ICP-AES, AAS
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