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- E-ISSN 2288-8985
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Simultaneous analysis of β-lactam antibiotics in surface water
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2010, v.23 no.2, pp.119-127
https://doi.org/10.5806/AST.2010.23.2.119
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(2010). Simultaneous analysis of β-lactam antibiotics in surface water. Analytical Science and Technology, 23(2), 119-127, https://doi.org/10.5806/AST.2010.23.2.119
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Abstract
An effective method for the simultaneous analysis of β-lactams from surface water was established. After solid-phase extraction with HLB (Hydrophilic Lipohilic Balance) cartridge at pH 2, seven β-lactams (amoxicillin, ampicillin, penicillin G, cefaclor, cefadroxil, cefatrizine and cephradine) were determined using LC/ESI-MS/MS. In this newly established method, correlation coefficients (r2) of calibration curves for seven β-lactams in blank surface water appeared to be 0.9911~0.9995 in the concentration range of 0.01~1.0 ng/mL. The limits of detection (LODs) and the limits of quantificaiton (LOQs) in spiked surface water were shown to be 0.0003~0.0234 ng/mL and 0.0046~0.0778 ng/mL, respectively. The developed method is believed to serve as a rapid and reliable method for the qualitative and quantitative analysis of residual β-lactam antibiotics from aquatic environment.
- keywords
- <TEX>${\beta}$</TEX>-lactam, surface water, LC/MS/MS, residual analysis
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