- P-ISSN 1225-0163
- E-ISSN 2288-8985
- P-ISSN1225-0163
- E-ISSN2288-8985
- SCOPUS, ESCI, KCI
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Determination of bromate in bottled mineral water in Korea
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
2010, v.23 no.2, pp.155-160
https://doi.org/10.5806/AST.2010.23.2.155
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(2010). Determination of bromate in bottled mineral water in Korea. Analytical Science and Technology, 23(2), 155-160, https://doi.org/10.5806/AST.2010.23.2.155
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Abstract
This study was performed to compare international analytical methods of bromate and applied to determine bromate in bottled mineral water in Korea. Bromate in bottled mineral water was eluted by 10~50mM potassium hydroxide (KOH) and determined by ion chromatograph-suppressed conductivity detector (ICCD). Sample was purified with on guard Ba-, Ag- and H-cartridges and 0.2 μm membrane filter. The method detection limit (MDL) and the limit of quantitation (LOQ) of bromate were 0.1 and 0.5 μg/L, respectively. The calibration curve showed good lineality above 0.9998 in the ranges of the 0.5~40 μg/L. Bromate from 33 samples among total 157 bottled mineral water samples was detected in the concentration range of 0.5~6.5μg/L. The detected concentrations were within bottled mineral water quality criteria (10 μg/L) in Korea.
- keywords
- bromate, IC-CD, bottled mineral water
Reference
1
1. K. C. Thompson, J. L. Guinamant, V. Ingrand, A. R. Elwaer, C. W. McLeod, F. Schmitz, G. De Swaef and Ph. Quevauviller, J. Environmental Monitoring, 2, 416- 419(2000).
2
2. M. Manassis and S. Constantinos, Ozone science & engineering, 25, 167-175(2002).
3
3. IARC, ‘Agents Reviewed by the IARC Monographs’, 1-100A(2009).
4
4. WHO, ‘Guidelines for Drinking Water Quality’, Geneva, Switzerland, 1993.
5
5. US EPA, Fed. Reg. 68(159), 49647, 2003.
6
6. WHO, ‘Guidelines for Drinking Water Quality’, Geneva, Switzerland, 2008.
7
7. US EPA, Fed. Reg. 66(60), 16858, 2001.
8
8. US EPA, ‘EPA method 300.1 The determination of Inorganic Anions in Water by Ion Chromatography’ Washington DC, US Environmental Protection Agency, 1997.
9
9. US EPA, ‘EPA method 317.0 Determination of Inorganic Oxyhalide Disinfection By-products in Drinking Water Using Ion Chromatography with the Addition of a Postcolumn Reagent for Trace Bromate Analysis’ Washington DC, US Environmental Protection Agency, 2001.
10
10. US EPA, ‘EPA method 326.1 Determination of Inorganic Oxyhalide Disinfection By-products in Drinking Water Using Ion Chromatography Incorporating the Addition of a Suppressor Acidified Postcolumn Reagent for Trace Bromate Analysis’, Washington DC, US Environmental Protection Agency, 2002.
11
11. US EPA, ‘EPA method 321.8 Determination of Bromate Ions in Waters Using Ion Chromatography with Inductively Coupled Plasma Mass Spectrometry’, Washington DC, US Environmental Protection Agency, 1997.
12
12. R. Michalski, Polish J. of Environ. Studies, 14(3), 257- 268(2005).
13
13. 한국표준협회, ‘KS I ISO 15061, 수질-용해된 브롬산염 측정-액상 이온 크로마토그래피법’, 2006.
14
14. B. M. De Borba, J. S. Rohrer, C. A. Pohl, C. Saini, J of Chromatogr. A, 1085, 23-32(2005).
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