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- E-ISSN 2288-8985
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Silicone Rubber Blended with Polyurethane as the Matrix for Ion-Selective Membrane Electrodes
Analytical Science and Technology / Analytical Science and Technology, (P)1225-0163; (E)2288-8985
1995, v.8 no.4, pp.623-630
Lee,
H. J., Rho,
K. L., Kim,
C. Y., Oh,
B. K., Cha,
G. S., &
Nam,
H.
(1995). Silicone Rubber Blended with Polyurethane as the Matrix for Ion-Selective Membrane Electrodes. Analytical Science and Technology, 8(4), 623-630.
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Abstract
Silicone rubber-based sodium-selective membranes are developed for solid-state ion sensors. It was shown that the potetiometric performance of SR-based membranes are greatly dependent on the type of neutral carriers employed; among the three ionophores, N,N,N',N'-tetracyclohexyl-1,2-phenylenedioxydiacetamide (ETH 2120), bis[(12-crown-4)methyl]dodecylmethylmalonate (D12C4DMM) and monensin methyl ester (MME), examined, only ETH 2120 was compatible with the SR-based matrix. Addition of about 20 wt% plasticizer to the SR-based matrix provided the resulting membranes with potentiometric properties essentially equivalent to those of the corresponding PVC-based membranes. Owing to the strong adhesive strength of SR-based membranes, the CWEs coated \vith those membranes exhibited long lifetime with conventional electrode-like performance. Blending of PU into the SR matrix increased the lifetime of CWEs from two weeks to one month.
- keywords
- ion-selective electrode, solid-state electrode, coated wire electrode (CWE), ISFET, silicone rubber matrix, polyurethane matrix, sodium-selective electrode
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